HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Heptylbenzoyl chloride → N-{4-[(4-chlorophenyl)ethynyl]benzyl)-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)-4-heptylbenzamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Heptylbenzoyl chloride | HCID 170864 | — |
| Reactant | 6-({4-[(4-chlorophenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one | HCID 11154301 | — |
| Product | N-{4-[(4-chlorophenyl)ethynyl]benzyl)-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)-4-heptylbenzamide | HCID 57841350 | — |
Reaction Steps
The titled compound was prepared following the procedure E using 6-({4-[(4-chlorophenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one and 4-heptylbenzoyl chloride as a yellow oil (94%). HPLC, Rt: 6.8 min (Purity: 96.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-049e166b3eaf4e68a2d92ac067315d83 |
| Source note | uspto-grants-2009_09 |