HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isoxazole-5-carbonyl chloride → HCID 57841414, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isoxazole-5-carbonyl chloride | HCID 2736707 | — |
| Reactant | 6-({4-[(4-chlorophenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one | HCID 11154301 | — |
| Product | HCID 57841414 | HCID 57841414 | — |
Reaction Steps
The titled compound was prepared following the procedure E using 6-({4-[(4-chlorophenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one and isoxazole-5-carbonyl chloride as a yellow oil (72%). M− (ESI): 511.5; M+ (ESI): 513.1. HPLC, Rt: 5.38 min (Purity: 99.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-fcf5415550f34884ab70a8685f5c2d35 |
| Source note | uspto-grants-2009_09 |