HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 11397323, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | N-(4-[(4-chlorophenyl)ethynyl]benzyl}-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)isoxazole-5-carboxamide | HCID 57841414 | — |
| Product | HCID 11397323 | HCID 11397323 | — |
Reaction Steps
The titled compound was prepared following the procedure C using N-{4-[(4-chlorophenyl)ethynyl]benzyl}-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)isoxazole-5-carboxamide and NaOH as a yellow solid (55%). M− (ESI): 470.7; M+ (ESI): 472.6. HPLC, Rt: 4.56 min (Purity: 71.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-0a75c3de3a8a4eb2bb06ab7d8c663641 |
| Source note | uspto-grants-2009_09 |