HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzoyl chloride → HCID 57841336, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzoyl chloride | HCID 74376 | — |
| Reactant | 6-({4-[(4-chlorophenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one | HCID 11154301 | — |
| Product | HCID 57841336 | HCID 57841336 | — |
Reaction Steps
The titled compound was prepared following the procedure E using 6-({4-[(4-chlorophenyl)ethynyl]benzyl}amino)-2,2-dimethyl-4H-1,3-benzodioxin-4-one and 3-fluorobenzoyl chloride as a yellow oil (96%). M+ (ESI): 540.2. HPLC, Rt: 5.71 min (Purity: 97.4%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-71c98fbd65e943999e1340b42f44e1f9 |
| Source note | uspto-grants-2009_09 |