Sodium Hydroxide → HCID 11181565, compound

Participants

Reaction Steps

The titled compound was prepared following the procedure C using N-{4-[(4-chlorophenyl)ethynyl]benzyl}-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-6-yl)-3-fluorobenzamide and NaOH as a white powder (56%). 1H NMR (MeOD, 300 MHz) δ 7.51 (m, 5H), 7.45-7.22 (m, 5H), 7.20-7.02 (m, 4H), 6.79 (d, J=9 Hz, 1H), 5.15 (s, 2H) M− (ESI): 497.9. HPLC. Rt: 4.92 min (Purity: 97.9%).

Provenance & Evidence