HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Cyclopentylpropionyl chloride → N-(4-bromobenzyl)-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Cyclopentylpropionyl chloride | HCID 66039 | — |
| Reactant | 7-[(4-bromobenzyl)amino]-2,2-dimethyl-4H-1,3-benzodioxin-4-one | HCID 57841387 | — |
| Product | N-(4-bromobenzyl)-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide | HCID 57841396 | — |
Reaction Steps
The titled compound was prepared following the procedure M using 7-[(4-bromobenzyl)amino]-2,2-dimethyl-4H-1,3-benzodioxin-4-one and 3-cyclopentylpropionyl chloride as a white powder (86%). M+ (ESI): 488.0. HPLC, Rt: 5.41 min (Purity: 99.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-74f919c50ce34e87b1ca7d4aeb793567 |
| Source note | uspto-grants-2009_09 |