HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-tert-Butylphenylacetylene → N-{4-[(4-tert-butylphenyl)ethynyl]benzyl}-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-tert-Butylphenylacetylene | HCID 2757302 | — |
| Reactant | N-(4-bromobenzyl)-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide | HCID 57841396 | — |
| Product | N-{4-[(4-tert-butylphenyl)ethynyl]benzyl}-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide | HCID 57841343 | — |
Reaction Steps
The titled compound was prepared following the procedure N using N-(4-bromobenzyl)-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide and 4-(tert-butyl)-phenylacetylene as a beige powder (65%). M1(ESI): 564.2. HPLC, Rt: 6.39 min (Purity: 98.9%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-6ecbaa5497874e98abacc77d3c665988 |
| Source note | uspto-grants-2009_09 |