HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Ethynyl-4-propoxybenzene → 3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)-N-{4-[(4-propoxyphenyl)ethynyl]benzyl}propanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Ethynyl-4-propoxybenzene | HCID 2775123 | — |
| Reactant | N-(4-bromobenzyl)-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide | HCID 57841396 | — |
| Product | 3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)-N-{4-[(4-propoxyphenyl)ethynyl]benzyl}propanamide | HCID 57841355 | — |
Reaction Steps
The titled compound was prepared following the procedure N using N-(4-bromobenzyl)-3-cyclopentyl-N-(2,2-dimethyl-4-oxo-4H-1,3-benzodioxin-7-yl)propanamide and 4-(propoxy)-phenylacetylene as a beige powder (59%). M+ (ESI): 566.2. HPLC, Rt: 6.17 min (Purity: 97.7%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589232B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d4799322ba874799bc66d3a3dd5a8c9e |
| Source note | uspto-grants-2009_09 |