HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,5-Difluoroaniline → HCID 57840950, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,5-Difluoroaniline | HCID 96595 | — |
| Reactant | HCID 57840951 | HCID 57840951 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 57840950 | HCID 57840950 | — |
Reaction Steps
Prepared in a similar manner to Example 4(d) from 4-tert-butylcarbamoyl-7-chloro-3-methyl-pyrrolo[2,3-c]pyridine-1-carboxylic acid ter-butyl ester (68 mg) and using 3,5-difluoroaniline (38 ul) instead of 3-bromoaniline. Isolated by MDAP rather than trituration with diethyl ether to give the title compound (28 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589206B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5ef0b24c683e4bce84c74521f0ef3277 |
| Source note | uspto-grants-2009_09 |