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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 733709Generated: October 30, 2026

Hydrochloric Acid → HCID 68868184, compound

https://huagongshe.com/reaction/733709

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57840894HCID 57840894—
CatalystDiethyl EtherHCID 3283—
SolventEthanolHCID 702—
ProductHCID 68868184HCID 68868184—

Reaction Steps

1-[7-(3-Fluoro-phenylamino)-1,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-4-yl]-1-morpholin-4-yl-methanone (73 mg) was dissolved in warm ethanol (12 ml) and treated with a solution of 1M hydrochloric acid in diethyl ether (10 drops) The mixture was evaporated, triturated with diethyl ether and filtered off then dried at 40° C. under vacuum to afford the title compound (65 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07589206B2
Source datasetuspto-grants-2009_09
ORD IDord-3f055bfb55c140ce889b5e2eaef9359d
Source noteuspto-grants-2009_09