HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 68869906, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 57841022 | HCID 57841022 | — |
| Catalyst | Diethyl Ether | HCID 3283 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 68869906 | HCID 68869906 | — |
Reaction Steps
1-[7-(3,5-Difluoro-phenylamino)-1,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-4-yl]-1-morpholin-4-yl-methanone (24 mg) was dissolved in warm ethanol (5 ml) and treated with a solution of 1M hydrochloric acid in diethyl ether (10 drops) The mixture was evaporated, triturated with diethyl ether and filtered off then dried at 40° C. under vacuum to afford the title compound (20 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589206B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-7b39ef28c16b4eeb910a8651b45411d3 |
| Source note | uspto-grants-2009_09 |