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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 733713Generated: October 28, 2026

Hydrochloric Acid → HCID 68869906, compound

https://huagongshe.com/reaction/733713

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57841022HCID 57841022—
CatalystDiethyl EtherHCID 3283—
SolventEthanolHCID 702—
ProductHCID 68869906HCID 68869906—

Reaction Steps

1-[7-(3,5-Difluoro-phenylamino)-1,3-dimethyl-1H-pyrrolo[2,3-c]pyridin-4-yl]-1-morpholin-4-yl-methanone (24 mg) was dissolved in warm ethanol (5 ml) and treated with a solution of 1M hydrochloric acid in diethyl ether (10 drops) The mixture was evaporated, triturated with diethyl ether and filtered off then dried at 40° C. under vacuum to afford the title compound (20 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07589206B2
Source datasetuspto-grants-2009_09
ORD IDord-7b39ef28c16b4eeb910a8651b45411d3
Source noteuspto-grants-2009_09