HRID733748

反应详情

EQUATION

反应方程式

HRID 733748 反应方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

N-(3-Chlorophenyl)-1-ethyl-7-(4-morpholinylcarbonyl)-1H-pyrrolo[3,2-c]pyridin-4-amine (14 mg) was dissolved in diethyl ether (2 ml) and 2M hydrochloric acid solution in diethyl ether added to give a solid precipitate. The diethyl ether was decanted off and the solid dried by evaporation to afford the title compound as a white powder (9 mg).

WORKUP

后处理

  1. customto give a solid precipitate
  2. customThe diethyl ether was decanted off
  3. customthe solid dried by evaporation