HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86615212, compound → HCID 86615213, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86615212 | HCID 86615212 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 86615213 | HCID 86615213 | 193.5% |
Reaction Steps
A solution of methyl 4-chloro-1,2-dimethyl-1H-pyrrolo[3,2-c]pyridine-7-carboxylate (1.027 g) in 5N hydrochloric acid was heated under microwave conditions at 120° C. for one and a half hours, then evaporated to dryness to afford the title compound as a white solid 1.087 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07589206B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-3ec97bda62d342d5b80fd44f2b33b3c4 |
| Source note | uspto-grants-2009_09 |