Hydrochloric Acid → HCID 68816388, compound

Participants

Reaction Steps

(S)-1-Isopropyl4-[1-(tert-butoxycarbonyl)-piperidine4-carbonyl]-3-methylpiperazine (D22)(0.11 g) was dissolved in methanol (10 ml) and treated with HCl (4N HCl in diethyl ether; 10 ml). After being stirred at rt overnight the reaction mixture was evaporated to a minimum, co-evaporated from methanol, and then dried at 50° C. to give the title compound (D23) as a pale brown solid (0.10 g)

Provenance & Evidence