Dimethylamine → 6-Chloro-N,N-dimethylnicotinamide

HRID 734340Notes

Reaction equation

[CH3:1][NH:2][CH3:3].[Cl:4][C:5]1[CH:13]=[CH:12][C:8]([C:9](O)=[O:10])=[CH:7][N:6]=1>>[Cl:4][C:5]1[CH:13]=[CH:12][C:8]([C:9]([N:2]([CH3:3])[CH3:1])=[O:10])=[CH:7][N:6]=1

Participants

Reactant 2

HCID 674Dimethylamine

HCID 792226-Chloronicotinic acid

Product 1

HCID 123642316-Chloro-N,N-dimethylnicotinamide

Procedure

The title compound (D36) was prepared from dimethylamine and 6-chloronicotinic acid according to the procedure described for Description 35. MS electrospray (+ve ion) 185 (MH+).

Sources & evidence

ORD record: ord-5e179311cd304fbebdf4b1d1ee747f38
Source dataset: uspto-grants-2009_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07592347B2

Reaction notes

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