HCID 68828054, compound → HCID 68827056, compound

HRID 734714Notes

Reaction equation

HRID 734714 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][C:12](=[O:14])[N:11]([CH3:15])[C:10]([CH3:16])=[C:9]2[C:17]([O:19]C)=[O:18])=[C:4]([F:21])[CH:3]=1>C1COCC1>[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([CH:8]2[CH2:13][C:12](=[O:14])[N:11]([CH3:15])[C:10]([CH3:16])=[C:9]2[C:17]([OH:19])=[O:18])=[C:4]([F:21])[CH:3]=1

Participants

3

Reactant 1

HCID 68828054HCID 68828054, compound

Product 1

HCID 68827056HCID 68827056, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The title compound was synthesized using the procedure stated in Example 1, Step 2 except that the product from Step 1 was used and THF was not used to yield product as an off white solid. MS (ES+) m/e 298 [M+H]+

Workup

  1. customto yield product as an off white solid

Sources & evidence

ORD record
ord-732c51c4f237407299f822a73d60c2a2
Source dataset
uspto-grants-2009_09
Patent number
US07592357B2

Reaction notes

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