Water → Decyl 4-bromobenzoate

HRID 73475Notes

Reaction equation

HRID 73475 reaction equation
C[C:2]1[CH:3]=[C:4]([C:8]2C=[CH:12][C:11](C(O)=O)=[CH:10][CH:9]=2)C=[CH:6][CH:7]=1.[Br:17][C:18]1[CH:26]=[CH:25][C:21]([C:22]([OH:24])=[O:23])=[CH:20][CH:19]=1.O>C1C=CC=CC=1>[Br:17][C:18]1[CH:26]=[CH:25][C:21]([C:22]([O:24][CH2:6][CH2:7][CH2:2][CH2:3][CH2:4][CH2:8][CH2:9][CH2:10][CH2:11][CH3:12])=[O:23])=[CH:20][CH:19]=1

Participants

5

Reactant 3

HCID 962WaterHCID 114644-Bromobenzoic acidHCID 27598163'-Methyl-biphenyl-4-carboxylic acid

Product 1

HCID 603107Decyl 4-bromobenzoate

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

Preparation of 3′-methyl-4-biphenylcarboxylic acid with OXO-C10 alcohols (NGP-87): Decyl 4-bromobenzoate was Prepared from the Condensation of 4-bromobenzoic acid and OXO-C10 alcohols by Refluxing in Benzene with Water Removal via a Dean-Stark Trap

Sources & evidence

ORD record
ord-cc67e74fe13c4716a860c8bba4fa54b3
Source dataset
uspto-grants-2014_09
Patent number
US08829093B2

Reaction notes

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