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HRID734794

反应详情

EQUATION

反应方程式

HRID 734794 的结构方程式

REACTANTS

反应物

1
结构：C[Si](C)(C)C#Cc1ccc(OCCO)cc1
HCID68473324

未命名化合物

PRODUCTS

生成物

1
结构：C#Cc1ccc(OCCO)cc1
HCID18751415

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

The product was obtained analogously to Example 1.1c starting from 12.20 g (52.05 mmol) of 2-(4-trimethylsilanylethynylphenoxy)ethanol. Yield: 7.70 g (91% of theoretical); C1oH10O2 (M=162.185); calc.: molpeak (M+H)+: 163; found: molpeak (M+H)+: 163; Rf value: 0.32 (silica gel, PE/EtOAc 6:4).

WORKUP

后处理

  1. customThe product was obtained analogously to Example 1.1c