HRID734796
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
产物
PROCEDURE
实验过程
The product was obtained analogously to Example 4.1f starting from 2-{4-[5-(4-chlorophenyl)pyridin-2-ylethynyl]phenoxy}ethyl methanesulfonate (Example 4.1e) and C-cyclopropylmethylamine. Yield: 700 mg (43% of theoretical); C25H23ClN2O (M=402.916); calc.: molpeak (M+H)+: 403/405 (Cl); found: molpeak (M+H)+: 403/405 (Cl); HPLC-MS: 5.08 minutes (method B).
WORKUP
后处理
- customThe product was obtained analogously to Example 4.1f
- custom5.08 minutes (method B)