HRID734796

反应详情

EQUATION

反应方程式

HRID 734796 反应方程式

PROCEDURE

实验过程

The product was obtained analogously to Example 4.1f starting from 2-{4-[5-(4-chlorophenyl)pyridin-2-ylethynyl]phenoxy}ethyl methanesulfonate (Example 4.1e) and C-cyclopropylmethylamine. Yield: 700 mg (43% of theoretical); C25H23ClN2O (M=402.916); calc.: molpeak (M+H)+: 403/405 (Cl); found: molpeak (M+H)+: 403/405 (Cl); HPLC-MS: 5.08 minutes (method B).

WORKUP

后处理

  1. customThe product was obtained analogously to Example 4.1f
  2. custom5.08 minutes (method B)