HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanemethanamine → HCID 69065035, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Reactant | HCID 86601132 | HCID 86601132 | — |
| Product | HCID 69065035 | HCID 69065035 | — |
Reaction Steps
The product was obtained analogously to Example 4.1f starting from 2-{4-[5-(4-chlorophenyl)pyridin-2-ylethynyl]phenoxy}ethyl methanesulfonate (Example 4.1e) and C-cyclopropylmethylamine. Yield: 700 mg (43% of theoretical); C25H23ClN2O (M=402.916); calc.: molpeak (M+H)+: 403/405 (Cl); found: molpeak (M+H)+: 403/405 (Cl); HPLC-MS: 5.08 minutes (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-38c9395fe713429bbdcb2941dbf5c02e |
| Source note | uspto-grants-2009_09 |