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HRID734803

反应详情

EQUATION

反应方程式

HRID 734803 的结构方程式

REACTANTS

反应物

2
结构：Cc1cc(I)ccc1OCCO
HCID4055115

未命名化合物

结构：C#Cc1ncc(-c2ccc(Cl)cc2)cc1F
HCID60055416

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C#Cc2ncc(-c3ccc(Cl)cc3)cc2F)ccc1OCCO
HCID69061948

未命名化合物

PROCEDURE

实验过程

The product was obtained analogously to Example 7.1e starting from 2-(4-iodo-2-methylphenoxy)ethanol and 5-(4-chlorophenyl)-2-ethynyl-3-fluoropyridine. Yield: 1.40 g (68% of theoretical); C22H17ClFNO2 (M=381.827); calc.: molpeak (M+H)+: 382/384 (Cl); found: molpeak (M+H)+: 382/384 (Cl); HPLC-MS: 6.29 minutes (method B).

WORKUP

后处理

  1. customThe product was obtained analogously to Example 7.1e
  2. custom6.29 minutes (method B)