HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 69064853, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69059991 | HCID 69059991 | — |
| Product | HCID 69064853 | HCID 69064853 | — |
Reaction Steps
The product was obtained analogously to Example 7.1e starting from 2-(4-iodo-2-vinylphenoxy)ethanol and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 0.66 g (96% of theoretical); C23H18ClNO2 (M=375.847); calc.: molpeak (M+H)+: 376/378 (Cl); found: molpeak (M+H)+: 376/378 (Cl); HPLC-MS: 6.21 minutes (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-3a0f2790978d4358803775961e265534 |
| Source note | uspto-grants-2009_09 |