HuagongsheHuagongshe Chemistry Print Report · For research reference only
BROMINE CHLORIDE (BrCl) → HCID 69057764, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | BROMINE CHLORIDE (BrCl) | HCID 61697 | — |
| Reactant | Trimethylsilylacetylene | HCID 66111 | — |
| Reactant | 2,3-Dibromo-5-(4-chlorophenyl)pyridine | HCID 86077043 | — |
| Product | HCID 69057764 | HCID 69057764 | — |
Reaction Steps
The product was prepared analogously to Example 7.1b starting from 2,3-dibromo-5-(4-chlorophenyl)pyridine and trimethylsilylacetylene. Yield: 1.00 g (95% of theoretical); C16H15BrClNSi (M=364.739); calc.: molpeak (M+H)+: 364/366/368 (BrCl); found: molpeak (M+H)+: 364/366/368 (BrCl).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-31e834c6425343c8a95011f90d5c9aac |
| Source note | uspto-grants-2009_09 |