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HRID734816

反应详情

EQUATION

反应方程式

HRID 734816 的结构方程式

REACTANTS

反应物

3
结构：ClBr
HCID61697

Bromine chloride (BrCl)

BrCl

2 次

结构：C#C[Si](C)(C)C
HCID66111

Trimethylsilylacetylene

C5H10Si

结构：Clc1ccc(-c2cnc(Br)c(Br)c2)cc1
HCID86077043

未命名化合物

PRODUCTS

生成物

1
结构：C[Si](C)(C)C#Cc1ncc(-c2ccc(Cl)cc2)cc1Br
HCID69057764

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1b starting from 2,3-dibromo-5-(4-chlorophenyl)pyridine and trimethylsilylacetylene. Yield: 1.00 g (95% of theoretical); C16H15BrClNSi (M=364.739); calc.: molpeak (M+H)+: 364/366/368 (BrCl); found: molpeak (M+H)+: 364/366/368 (BrCl).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1b