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HRID734817

反应详情

EQUATION

反应方程式

HRID 734817 的结构方程式

REACTANTS

反应物

2
结构：ClBr
HCID61697

Bromine chloride (BrCl)

BrCl

2 次

结构：C[Si](C)(C)C#Cc1ncc(-c2ccc(Cl)cc2)cc1Br
HCID69057764

未命名化合物

PRODUCTS

生成物

1
结构：C#Cc1ncc(-c2ccc(Cl)cc2)cc1Br
HCID86077051

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1d starting from 3-bromo-5-(4-chlorophenyl)-2-trimethylsilanylethynylpyridine. Yield: 0.44 g (55% of theoretical); C13H7BrClN (M=292.558); calc.: molpeak (M+H)+: 292/294/296 (BrCl); found: molpeak (M+H)+: 292/294/296 (BrCl); HPLC-MS: 6.21 minutes (method B).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1d
  2. custom6.21 minutes (method B)