huagongshe.com
HRID734823

反应详情

EQUATION

反应方程式

HRID 734823 的结构方程式

REACTANTS

反应物

2
结构：CC1CCN(CCOc2ccc(I)cc2)CC1
HCID69061017

未命名化合物

结构：C#Cc1ncc(-c2ccc(Cl)cc2)cc1N
HCID86077060

未命名化合物

PRODUCTS

生成物

1
结构：CC1CCN(CCOc2ccc(C#Cc3ncc(-c4ccc(Cl)cc4)cc3N)cc2)CC1
HCID11496018

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1e starting from 5-(4-chlorophenyl)-2-ethynylpyridin-3-ylamine and 1-[2-(4-iodophenoxy)ethyl]-4-methylpiperidine. Yield: 0.63 (75% of theoretical); C27H28ClN3O (M=445.984); calc.: molpeak (M+H)+: 446/448 (Cl); found: molpeak (M+H)+: 446/448 (Cl); HPLC-MS: 5.05 minutes (method D).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1e
  2. custom5.05 minutes (method D)