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HRID734826

反应详情

EQUATION

反应方程式

HRID 734826 的结构方程式

REACTANTS

反应物

2
结构：C#Cc1ccc(-c2ccc(Cl)cc2)cn1
HCID57845328

未命名化合物

结构：Cc1cc(I)ccc1NCCN1CCC(C)CC1
HCID69059102

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(C#Cc2ccc(-c3ccc(Cl)cc3)cn2)ccc1NCCN1CCC(C)CC1
HCID11597445

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1e starting from (4-iodo-2-methylphenyl)-[2-(4-methylpiperidin-1-yl)ethyl]amine and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 60 mg (20% of theoretical); C28H30ClN3 (M=444.011); calc.: molpeak (M+H)+444/446 (Cl); found molpeak (M+H)+: 444/446 (Cl); HPLC-MS: 5.53 minutes (method B).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1e
  2. custom5.53 minutes (method B)