HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 11597445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | (4-Iodo-2-methylphenyl)-[2-(4-methylpiperidin-1-yl)ethyl]amine | HCID 69059102 | — |
| Product | HCID 11597445 | HCID 11597445 | — |
Reaction Steps
The product was prepared analogously to Example 7.1e starting from (4-iodo-2-methylphenyl)-[2-(4-methylpiperidin-1-yl)ethyl]amine and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 60 mg (20% of theoretical); C28H30ClN3 (M=444.011); calc.: molpeak (M+H)+444/446 (Cl); found molpeak (M+H)+: 444/446 (Cl); HPLC-MS: 5.53 minutes (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-d64a8ceae1154d1ea6c36efa505e7c59 |
| Source note | uspto-grants-2009_09 |