HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trimethylsilylacetylene → HCID 69058638, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trimethylsilylacetylene | HCID 66111 | — |
| Reactant | HCID 86077064 | HCID 86077064 | — |
| Product | HCID 69058638 | HCID 69058638 | — |
Reaction Steps
The product was obtained analogously to Example 7.1b starting from 2-bromo-3-chloro-5-(4-chlorophenyl)pyridine and trimethylsilylacetylene. Yield: 0.57 g (quant. yield); C16H15Cl2NSi (M=320.288); calc.: molpeak (M+H)+: 320/322/324 (2Cl); found: molpeak (M+H)+: 320/322/324 (2Cl); HPLC-MS: 8.02 minutes (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-2d2e0db962c34f0eb58ae17f70a2f6c7 |
| Source note | uspto-grants-2009_09 |