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HRID734828

反应详情

EQUATION

反应方程式

HRID 734828 的结构方程式

REACTANTS

反应物

2
结构：OCCOc1ccc(I)cc1
HCID3513208

未命名化合物

结构：C#Cc1ncc(-c2ccc(Cl)cc2)cc1Cl
HCID86077065

未命名化合物

PRODUCTS

生成物

1
结构：OCCOc1ccc(C#Cc2ncc(-c3ccc(Cl)cc3)cc2Cl)cc1
HCID69059827

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1e starting from 3-chloro-5-(4-chlorophenyl)-2-ethynylpyridine and 2-(4-iodophenoxy)ethanol. Yield: 0.48 g (66% of theoretical); C21H15Cl2NO2 (M=384.255); calc.: molpeak (M+H)+384/386/388 (2Cl); found: molpeak (M+H)+: 384/386/388 (2Cl); HPLC-MS: 6.24 minutes (method B).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1e
  2. custom6.24 minutes (method B)