HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Iodophenoxy)ethanol → HCID 69059827, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Iodophenoxy)ethanol | HCID 3513208 | — |
| Reactant | 3-Chloro-5-(4-chlorophenyl)-2-ethynylpyridine | HCID 86077065 | — |
| Product | HCID 69059827 | HCID 69059827 | — |
Reaction Steps
The product was prepared analogously to Example 7.1e starting from 3-chloro-5-(4-chlorophenyl)-2-ethynylpyridine and 2-(4-iodophenoxy)ethanol. Yield: 0.48 g (66% of theoretical); C21H15Cl2NO2 (M=384.255); calc.: molpeak (M+H)+384/386/388 (2Cl); found: molpeak (M+H)+: 384/386/388 (2Cl); HPLC-MS: 6.24 minutes (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b6c812566d88441585d846c95170540d |
| Source note | uspto-grants-2009_09 |