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HRID734841

反应详情

EQUATION

反应方程式

HRID 734841 的结构方程式

REACTANTS

反应物

2
结构：C#Cc1ccc(Br)cn1
HCID13979734

5-Bromo-2-ethynylpyridine

C7H4BrN

结构：CC1CCN(CCOc2ccc(I)cc2)CC1
HCID69061017

未命名化合物

PRODUCTS

生成物

1
结构：CC1CCN(CCOc2ccc(C#Cc3ccc(Br)cn3)cc2)CC1
HCID69060172

未命名化合物

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1e starting from 1-[2-(4-iodophenoxy)ethyl]-4-methylpiperidine and 5-bromo-2-ethynylpyridine. Yield: 1.00 g (62% of theoretical); C21H23BrN2O (M=399.324); calc.: molpeak (M+H)+: 399/401 (Br); found: molpeak (M+H)+: 399/401 (Br); HPLC-MS: 4.64 minutes (method A).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1e
  2. custom4.64 minutes (method A)