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HRID734845

反应详情

EQUATION

反应方程式

HRID 734845 的结构方程式

REACTANTS

反应物

2
结构：CC1CCN(CCN)CC1
HCID783700

2-(4-methylpiperidin-1-yl)ethanamine

C8H18N2

结构：Clc1ccc(-c2ccc(C#Cc3cc(I)cs3)nc2)cc1
HCID69056001

未命名化合物

PRODUCTS

生成物

1
结构：CC1CCN(CCNc2csc(C#Cc3ccc(-c4ccc(Cl)cc4)cn3)c2)CC1
HCID57845298

未命名化合物

PROCEDURE

实验过程

The product was obtained analogously to Example 20.1a starting from 5-(4-chlorophenyl)-2-(4-iodothiophen-2-ylethynyl)pyridine and 2-(4-methylpiperidin-1-yl)ethylamine. Yield: 3 mg (1% of theoretical); C25H26ClN3S (M=436.013); calc.: molpeak (M+H)+: 436/438 (Cl); found: molpeak (M+H)+: 436/438 (Cl); HPLC-MS: 5.10 minutes (method B).

WORKUP

后处理

  1. customThe product was obtained analogously to Example 20.1a
  2. custom5.10 minutes (method B)