HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 57845334, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69061391 | HCID 69061391 | — |
| Product | HCID 57845334 | HCID 57845334 | — |
Reaction Steps
The product was obtained analogously to Example 7.1e starting from 5-iodo-2-(2-pyrrolidin-1-ylethoxy)benzylamine and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 28 mg (11% of theoretical); C26H26ClN3O (M=431.957); calc.: molpeak (M+H)+: 432/434 (Cl); found: molpeak (M+H)+: 432/434 (Cl); HPLC-MS: 3.90 minutes (method B).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-3470fcb32d504ce68c19a92f8b97961e |
| Source note | uspto-grants-2009_09 |