HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 57845309, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69061413 | HCID 69061413 | — |
| Product | HCID 57845309 | HCID 57845309 | — |
Reaction Steps
The product was obtained analogously to Example 7.1e starting from 5-iodo-2-(2-pyrrolidin-1-ylethoxy)phenol and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 0.75 g (48% of theoretical); C25H23ClN2O2 (M=418.915); calc.: molpeak (M+H)+: 419/421 (Cl); found: molpeak (M+H)+: 419/421 (Cl); HPLC-MS: 7.33 minutes (method A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-b1559f8104774836a3dce911a05f1fc1 |
| Source note | uspto-grants-2009_09 |