HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 69059110, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69065025 | HCID 69065025 | — |
| Product | HCID 69059110 | HCID 69059110 | — |
Reaction Steps
The product was obtained analogously to Example 7.1e starting from 3-(5-iodopyridin-2-yl)propan-1-ol and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 0.80 g (74% of theoretical); C21H17ClN2O (M=348.825); calc.: molpeak (M+H)+: 349/351 (Cl); found: molpeak (M+H)+: 349/351 (Cl); HPLC-MS: 8.24 minutes (method A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-93e3d3903fe44fcd8be0ebea738418bd |
| Source note | uspto-grants-2009_09 |