HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-4-iodobenzene → HCID 69057479, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-4-iodobenzene | HCID 11522 | — |
| Reactant | BROMINE CHLORIDE (BrCl) | HCID 61697 | — |
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Product | HCID 69057479 | HCID 69057479 | — |
Reaction Steps
The product was obtained analogously to Example 7.1e starting from 4-bromoiodobenzene and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 7.10 g (90% of theoretical); C19H11BrClN (M=368.654); calc.: molpeak (M+H)+: 368/370/372 (BrCl); found: molpeak (M+H)+: 368/370/372 (BrCl); HPLC-MS: 7.60 minutes (method A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-37c3ca2b66094d86a383f3f7f36f1368 |
| Source note | uspto-grants-2009_09 |