HRID734872

反应详情

EQUATION

反应方程式

HRID 734872 的结构方程式

PROCEDURE

实验过程

The product was prepared analogously to Example 7.1e starting from 1-[2-(4-iodophenoxy)ethyl]-4-methylpiperidine and [5-(4-chlorophenyl)-2-ethynylpyridin-3-yl]methylamine. Yield: 70 mg (21% of theoretical); C28H30ClN3O (M=460.010); calc.: molpeak (M+H)+:460/462 (Cl); found: molpeak (M+H)+:460/462 (Cl); HPLC-MS: 5.30 minutes (method D).

WORKUP

后处理

  1. customThe product was prepared analogously to Example 7.1e
  2. custom5.30 minutes (method D)