HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(4-Chloro-phenyl)-2-ethynyl-pyridine → HCID 69058833, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(4-Chloro-phenyl)-2-ethynyl-pyridine | HCID 57845328 | — |
| Reactant | HCID 69056726 | HCID 69056726 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 69058833 | HCID 69058833 | — |
Reaction Steps
The product was obtained analogously to Example 7.1e starting from 4-(4-iodophenyl)piperidin-4-ol and 5-(4-chlorophenyl)-2-ethynylpyridine. Yield: 0.78 g (61% of theoretical); C24H21ClN2O (M=388.889); calc.: molpeak (M+H)+:389/391 (Cl); found: molpeak (M+H)+:389/391 (Cl); Rf value: 0.86 (silica gel, EtOAc/cyc 4:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592358B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-668af006bef34e57a59f884c43f6774a |
| Source note | uspto-grants-2009_09 |