HRID734904

反应详情

EQUATION

反应方程式

HRID 734904 的结构方程式

PROCEDURE

实验过程

The product was prepared analogously to Example 50.5d from 100 mg (0.53 mmol) of (5-but-3-ynylpyridin-2-yl)isopropylamine and 168 mg (0.53 mmol) of 5-(4-chlorophenyl)-2-iodopyridine (purification by preparative HPLC-MS). Yield: 520 mg (54% of theoretical); C23H22ClN3 (M=375.894); calc.: molpeak (M+H)+:376/378; found: molpeak (M+H)+:376/378; HPLC-MS: 5.33 minutes (method G).

WORKUP

后处理

  1. custom5.33 minutes (method G)