huagongshe.com
HRID734995

反应详情

EQUATION

反应方程式

HRID 734995 的结构方程式

REACTANTS

反应物

2
结构：C#CC(=O)O
HCID10110

2-Propynoic acid

C3H2O2

结构：COc1ccc(-c2ccc(N)cc2)cc1
HCID2759564

4-(4-methoxyphenyl)aniline

C13H13NO

PRODUCTS

生成物

1
结构：C#CC(=O)Nc1ccc(-c2ccc(OC)cc2)cc1
HCID86060753

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO.ClCCl
溶剂HCID21584144

Dichloromethane ethanol

C3H8Cl2O

PROCEDURE

实验过程

Prepared analogously to Example 1.1.b. from propynoic acid and 4′-methoxybiphenyl-4-ylamine. Yield: 1.3 g (17.2% of theory); C16H13NO2 (M=251.28); calc.: molecular ion peak (M+H)+: 252; found: molecular ion peak (M+H)+: 252; Rf value: 0.6 (silica gel, dichloromethane/ethanol (20:1)).

WORKUP

后处理

  1. customPrepared analogously to Example 1.1.b