HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propiolic Acid → Propynoic acid-(4'-methoxybiphenyl-4-yl)amide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propiolic Acid | HCID 10110 | — |
| Reactant | 4-Amino-4'-methoxybiphenyl | HCID 2759564 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | Propynoic acid-(4'-methoxybiphenyl-4-yl)amide | HCID 86060753 | — |
Reaction Steps
Prepared analogously to Example 1.1.b. from propynoic acid and 4′-methoxybiphenyl-4-ylamine. Yield: 1.3 g (17.2% of theory); C16H13NO2 (M=251.28); calc.: molecular ion peak (M+H)+: 252; found: molecular ion peak (M+H)+: 252; Rf value: 0.6 (silica gel, dichloromethane/ethanol (20:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-222bdb2d172b437499dd0919b0f4b13a |
| Source note | uspto-grants-2009_09 |