HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 68816419, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Dichloromethane ethanol | HCID 21584144 | — |
| Reactant | HCID 86601886 | HCID 86601886 | — |
| Product | HCID 68816419 | HCID 68816419 | — |
Reaction Steps
Prepared analogously to Example 1.2.c. from 4-[(4′-methoxybipheny-4-ylcarbamoyl)ethynyl]benzyl methanesulfonate and piperidine. Yield: 5 mg (18.8% of theory); melting point: 170° C.; C28H28N2O2 (M=424.54); calc.: molecular ion peak (M+H)+: 425; found: molecular ion peak (M+H)+: 425; Rf value: 0.28 (silica gel, dichloromethane/ethanol (20:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-32460f4dc0864001925a784b5517f447 |
| Source note | uspto-grants-2009_09 |