HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(1-Pyrrolidinyl)piperidine → HCID 68816274, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(1-Pyrrolidinyl)piperidine | HCID 78703 | — |
| Reactant | 4-Iodobenzyl bromide | HCID 954258 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 68816274 | HCID 68816274 | — |
Reaction Steps
Prepared analogously to Example 1.1.c. from 4-iodobenzyl bromide and 4-pyrrolidin-1-ylpiperidine. Yield: 0.57 g (51% of theory); C16H23IN2 (M=370.28); calc.: molecular ion peak (M+H)+: 371; found: molecular ion peak (M+H)+: 371; Rf value: 0.3 (silica gel, dichloromethane/ethanol (20:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-5745d6df08134cf48749021b6f368408 |
| Source note | uspto-grants-2009_09 |