HRID735008

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID954258

4-Iodobenzyl bromide

C7H6BrI

HCID5200321

2-(Piperidin-4-yl)propan-2-ol

C8H17NO

PRODUCTS

生成物

HCID68816491

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21584144

Dichloromethane ethanol

C3H8Cl2O

PROCEDURE

实验过程

Prepared analogously to Example 1.1.c. from 4-iodobenzyl bromide and 2-piperidin-4-ylpropan-2-ol. Yield: 1.01 g (67% of theory); C15H22INO (M=359.25); calc.: molecular ion peak (M+H)+: 360; found: molecular ion peak (M+H)+: 360; Rf value: 0.4 (silica gel, dichloromethane/ethanol (20:1)).

WORKUP

后处理

customPrepared analogously to Example 1.1.c