HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodobenzyl bromide → HCID 68816491, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodobenzyl bromide | HCID 954258 | — |
| Reactant | 2-(4-Piperidyl)-2-propanol | HCID 5200321 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 68816491 | HCID 68816491 | — |
Reaction Steps
Prepared analogously to Example 1.1.c. from 4-iodobenzyl bromide and 2-piperidin-4-ylpropan-2-ol. Yield: 1.01 g (67% of theory); C15H22INO (M=359.25); calc.: molecular ion peak (M+H)+: 360; found: molecular ion peak (M+H)+: 360; Rf value: 0.4 (silica gel, dichloromethane/ethanol (20:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-dc8c9874e1ef49db95941d1ff542cb25 |
| Source note | uspto-grants-2009_09 |