HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methoxypiperidine → HCID 65478349, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methoxypiperidine | HCID 77666 | — |
| Reactant | 4-Iodobenzyl bromide | HCID 954258 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 65478349 | HCID 65478349 | — |
Reaction Steps
Prepared analogously to Example 1.1.c. from 4-iodobenzyl bromide and 4-methoxypiperidine. Yield: 0.93 g (66.7% of theory); C13H18INO (M=331.19); calc.: molecular ion peak (M+H)+: 332; found: molecular ion peak (M+H)+: 332; Rf value: 0.55 (silica gel, dichloromethane/ethanol (20:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-0f2556df002744ce8325eb2589009294 |
| Source note | uspto-grants-2009_09 |