HRID735013

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID954258

4-Iodobenzyl bromide

C7H6BrI

HCID15649174

4-Methylpiperidin-4-ol

C6H13NO

PRODUCTS

生成物

HCID68816798

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID21584144

Dichloromethane ethanol

C3H8Cl2O

PROCEDURE

实验过程

Prepared analogously to Example 1.1.c. from 4-iodobenzyl bromide and 4-methylpiperidin-4-ol. Yield: 0.22 g (30% of theory); C13H18INO (M=331.19); calc.: molecular ion peak (M+H)+: 332; found: molecular ion peak (M+H)+: 332; Rf value: 0.45 (silica gel, dichloromethane/ethanol (20:1)).

WORKUP

后处理

customPrepared analogously to Example 1.1.c