HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Iodobenzyl bromide → HCID 68816798, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Iodobenzyl bromide | HCID 954258 | — |
| Reactant | 4-Methylpiperidin-4-ol | HCID 15649174 | — |
| Solvent | Dichloromethane ethanol | HCID 21584144 | — |
| Product | HCID 68816798 | HCID 68816798 | — |
Reaction Steps
Prepared analogously to Example 1.1.c. from 4-iodobenzyl bromide and 4-methylpiperidin-4-ol. Yield: 0.22 g (30% of theory); C13H18INO (M=331.19); calc.: molecular ion peak (M+H)+: 332; found: molecular ion peak (M+H)+: 332; Rf value: 0.45 (silica gel, dichloromethane/ethanol (20:1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-edab6f259c0e43d6bd37e16c6cd924f1 |
| Source note | uspto-grants-2009_09 |