HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(4-Iodobenzyl)piperidine → HCID 57845766, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(4-Iodobenzyl)piperidine | HCID 7537600 | — |
| Reactant | Ammonia methanol dichloromethane | HCID 21584172 | — |
| Reactant | Propynoic acid-(4'-chlorobiphenyl-4-yl)amide | HCID 86060771 | — |
| Product | HCID 57845766 | HCID 57845766 | — |
Reaction Steps
Prepared analogously to Example 1.1.d. from 1-(4-iodobenzyl)piperidine and propynoic acid-(4′-chlorobiphenyl-4-yl)amide. Yield: 6 mg (4% of theory); melting point: 179.5° C.; C27H25ClN2O (M=428.96); calc.: molecular ion peak (H+ H)+: 429/431; found: molecular ion peak (M+H)+: 429/431; Rf value: 0.5 (silica gel, dichloromethane/methanol/ammonia (10:1:0.1)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07592373B2 |
| Source dataset | uspto-grants-2009_09 |
| ORD ID | ord-0f29346000d944878000fb1fbd0c39a5 |
| Source note | uspto-grants-2009_09 |